Abstract

ISO 18363 specifies a procedure for the simultaneous determination of 2-MCPD esters (bound 2-MCPD), 3-MCPD esters (bound 3-MCPD) and glycidyl esters (bound glycidol) in a single assay, based on acid catalysed ester cleavage and derivatization of cleaved (free) analytes with phenylboronic acid (PBA) prior to GC/MS analysis. ISO 18363-3 is applicable to solid and liquid fats and oils. For all three analytes the limit of quantification (LOQ) is 0,1 mg/kg and the limit of detection (LOD) is 0,03 mg/kg.

Begin

2023-12-11

WI

00307204

Planned document number

DIN EN ISO 18363-3

Project number

05702704

Responsible national committee

NA 057-05-05 AA - Joint committee of DIN and DGF for the analysis of fats, oils and products thereof, related and primary products  

Responsible european committee

CEN/TC 307 - Oilseeds, vegetable and animal fats and oils and their by-products - Methods of sampling and analysis  

Responsible international committee

ISO/TC 34/SC 11 - Animal and vegetable fats and oils  

draft standard

Animal and vegetable fats and oils - Determination of fatty-acid-bound chloropropanediols (MCPDs) and glycidol by GC/MS - Part 3: Method using acid transesterification and measurement for 2-MCPD, 3-MCPD and glycidol (ISO/FDIS 18363-3:2024); German and English version prEN ISO 18363-3:2024
2024-05
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previous edition(s)

Animal and vegetable fats and oils - Determination of fatty-acid-bound chloropropanediols (MCPDs) and glycidol by GC/MS - Part 3: Method using acid transesterification and measurement for 2-MCPD, 3-MCPD and glycidol (ISO 18363-3:2017); German version EN ISO 18363-3:2021
2022-04

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